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Mass spectrometric analysis of the volatiles released by heating or crushing rocksVacuum extraction with subsequent mass spectrometric analysis of evolved volatiles was selected as the analytical procedure. The high-vacuum gas-handling system was constructed of stainless steel. The system was completely free from mercury, grease, or volatile organic materials. The furnace for heating the samples is discussed together with the high-vacuum crusher, the mass spectrometer, and approaches for water determination. The analytical procedure is considered, giving attention to the extraction of volatiles, adsorption studies, and the analysis of volatiles.
Document ID
19740027766
Acquisition Source
Legacy CDMS
Document Type
Conference Proceedings
Authors
Barker, C. (Tulsa, University Tulsa, Okla., United States)
Sommer, M. A.
Date Acquired
August 7, 2013
Publication Date
January 1, 1973
Subject Category
Chemistry
Meeting Information
Meeting: Symposium on the Analytical methods developed for application to lunar samples analyses
Location: Los Angeles, CA
Start Date: June 25, 1972
End Date: June 30, 1972
Accession Number
74A10516
Funding Number(s)
CONTRACT_GRANT: NGR-37-008-002
Distribution Limits
Public
Copyright
Other

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