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Seeded Growth of Colloidal Silica ParticlesThe method of seeded growth was studied for producing mondisperse colloidal silica particles. It was shown that particle size as well as weight percent solids could be controlled by using this method. The particles were characterized by transmission electron microscopy (TEM) and quasielastic light scattering (QELS). The particles were found to have a bimodal size distribution when examined by TEM. The particle size as determined by QELS was found to be roughly 10-20% larger than the particle size as determined by TEM. Furthermore, the polydispersity (standard deviation/mean particle size) as determined by QELS was found to be significantly lower than the polydispersity as determined by TEM. This underscores the importance of using TEM as a characterization technique for determining particle monodispersity. It was also noted that there was an increase in particle roughness as the weight percent of the silica particles increased and a new nucleation of particles was observed as the weight percent approached 13%. A recipe for producing monodisperse silica particles in the 150 nm size range is presented.
Document ID
20020043211
Acquisition Source
Headquarters
Document Type
Other
Authors
Wurm, David B.
(University of Southeastern Louisiana Hammond, LA United States)
Date Acquired
August 20, 2013
Publication Date
October 1, 1999
Publication Information
Publication: 1999 NASA/ASEE Summer Faculty Fellowship Program
Subject Category
Nonmetallic Materials
Funding Number(s)
CONTRACT_GRANT: NGT8-52874
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.

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