Early lunar history - Ages of 2 to 4 mm soil fragments from the lunar highlands

The ages of twenty-one 2 to 4 mm soil fragments from Apollo 16 stations 6, 8, 11, and 13, including all six major petrographic rock types found among Apollo 16 samples, were determined using the Ar-40/Ar-39 stepwise-heating technique. Twelve of the twenty-one samples have ages within 3.95 to 4.06 billion years, and it is believed that they represent the age of at least one stage of the Cayley Formation. Four samples have ages distinctly older than 4.00 billion years, making them the oldest lunar material found to date.