Viscosity measuring instrument

A method and apparatus are provided for enabling the measurement of the viscosity of substances, especially those containing volatiles at elevated temperatures, with greater accuracy and at less cost than before. The apparatus includes a cylinder with a narrow exit opening at one end and a piston which closely slides within the cylinder to apply force against a sample in the cylinder to force the sample through the exit opening. In order to more rapidly heat a sample the ends of the cylinder and piston are tapered and the sample is correspondingly tapered, to provide a large surface to volume ratio. A corresponding coal sample is formed by compressing particles of coal under high pressure in a mold of appropriate shape.