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Method and apparatus for minimizing convection during crystal growth from solutionA method and apparatus are disclosed for growing in a gravitational field a microscopic crystal from a solution. The solution is held in a vertical chamber which is relatively thin, the thin being generally perpendicular to the vertical. There is a substrate crystal disposed at either the upper or lower end of the chamber and the crystal grows from this substrate crystal in one direction. The temperature conditions of the solution are controlled so that, as the crystal forms, the effects of buoyant convection within the solution are minimized. This is accomplished in two different ways depending upon whether the crystal is grown from the upper or lower end of the chamber. When grown from the upper end of the chamber, the temperature of the solution is controlled so that it remains essentially isothermal so that there is essentially no heat loss from the solution. When the crystal is grown from the lower end of the chamber, the temperature of the solution is controlled so that there is a differential in temperature throughout the solution which provides a positive thermal gradient within the chamber.
Document ID
19840004900
Acquisition Source
Legacy CDMS
Document Type
Other - Patent Application
Authors
Shlichta, P. J.
(JPL California Inst. of Tech., Pasadena, United States)
Date Acquired
September 4, 2013
Publication Date
October 31, 1983
Subject Category
Solid-State Physics
Report/Patent Number
Patent Number: NASA-CASE-NPO-15811-1
Patent Application Number: US-PATENT-APPL-SN-547175
Accession Number
84N12968
Funding Number(s)
CONTRACT_GRANT: NAS7-100
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.
Patent
NASA-CASE-NPO-15811-1
Patent Application
US-PATENT-APPL-SN-547175
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