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Mononitration of dureneReaction conditions under which the nitration of durene give predominantly, and in high yield, mononitrodurene (I), rather than dinitrodurene were found. The nitrating agent was No2+RF6-. Nitration with nitrosulfuric acid also gave mononitrodurene; however, byproducts such as 2.3.5.6-Me4C6HCH2C6H2Me3-2,4,5, were also formed. The NO2 PF6- gave an intermediate additional compound with durene. The reaction carried out with 3.6-dideuterodurene in D2O shows no isotope effect.
Document ID
19850006583
Acquisition Source
Legacy CDMS
Document Type
Technical Memorandum (TM)
Authors
Hanna, S. B. (NASA Headquarters Washington, DC United States)
Hunziker, E. (NASA Headquarters Washington, DC United States)
Saito, T. (NASA Headquarters Washington, DC United States)
Zollinger, H. (NASA Headquarters Washington, DC United States)
Date Acquired
September 5, 2013
Publication Date
December 1, 1984
Subject Category
Inorganic And Physical Chemistry
Report/Patent Number
NAS 1.15:77774
NASA-TM-77774
Report Number: NAS 1.15:77774
Report Number: NASA-TM-77774
Accession Number
85N14892
Funding Number(s)
CONTRACT_GRANT: NASW-4005
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.

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