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Process for producing tris s(n-methylamino) methylsilaneA method of producing tris (N-methylamine) methylsilane is described including the steps of forming and cooling a liquid solution of methylamine in an inert solvent and under an inert atmosphere at a temperature of about -30 C and slowly adding a quantity of methyltricholorosilane while maintaining said temperature. The reaction mixture is then heated for about 60 minutes at a temperature of about 40 C, followed by filtering the solid portion from the liquid portion. The liquid is distilled to remove the solvent, resulting in a high yield of tris (N-methylamine) methylsilane.
Document ID
19850012970
Acquisition Source
Legacy CDMS
Document Type
Other - Patent
Authors
Clemons, J. M.
(NASA Marshall Space Flight Center Huntsville, AL, United States)
Penn, B. G.
(NASA Marshall Space Flight Center Huntsville, AL, United States)
Ledbetter, F. E., III
(NASA Marshall Space Flight Center Huntsville, AL, United States)
Date Acquired
August 12, 2013
Publication Date
October 2, 1984
Subject Category
Inorganic And Physical Chemistry
Report/Patent Number
NAS 1.71:MFS-25721-1
Patent Number: NASA-CASE-MFS-25721-1
Patent Application Number: US-PATENT-APPL-SN-492964
Patent Number: US-PATENT-4,474,975
Report Number: NAS 1.71:MFS-25721-1
Accession Number
85N21280
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.
Patent
NASA-CASE-MFS-25721-1|US-PATENT-4,474,975
Patent Application
US-PATENT-APPL-SN-492964
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