Requirements and an approach for coating the Gravity Probe B gyroscope rotor

A process to coat a quartz gyroscope rotor uniformly with superconducting niobium as part of a NASA sponsored experiment to test general relativity is described. The requirements for uniformity, film adhesion, and superconducting properties of the niobium thin film rotor coating are discussed. A uniformity of 1.5 percent (peak to valley) (38 nm) with good adhesion, no pinholes larger than 0.25 mm, transition temperature of 9.8 K, and the ability to survive repeated thermal cycling to 4.2 K have been achieved. Problems concerning abrasive damage and electrical arc damage during earthbound testing have been observed. Many hours of ground-based gyro operation demonstrate the applicability of this approach to rotor coating.