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Device and method for measuring thermal conductivity of thin filmsA device and method are provided for measuring the thermal conductivity of rigid or flexible, homogeneous or heterogeneous, thin films between 50 .mu.m and 150 .mu.m thick with relative standard deviations of less than five percent. The specimen is sandwiched between like material, highly conductive upper and lower slabs. Each slab is instrumented with six thermocouples embedded within the slab and flush with their corresponding surfaces. A heat source heats the lower slab and a heat sink cools the upper slab. The heat sink also provides sufficient contact pressure onto the specimen. Testing is performed within a vacuum environment (bell-jar) between 10.sup.-3 to 10.sup.-6 Torr. An anti-radiant shield on the interior surface of the bell-jar is used to avoid radiation heat losses. Insulation is placed adjacent to the heat source and adjacent to the heat sink to prevent conduction losses. A temperature controlled water circulator circulates water from a constant temperature bath through the heat sink. Fourier's one-dimensional law of heat conduction is the governing equation. Data, including temperatures, are measured with a multi-channel data acquisition system. On-line computer processing is used for thermal conductivity calculations.
Document ID
20080004161
Acquisition Source
Headquarters
Document Type
Other - Patent
Authors
Amer, Tahani R.
Subramanian, Chelakara
Upchurch, Billy T.
Alderfer, David W.
Sealey, Bradley S.
Burkett, Jr., Cecil G.
Date Acquired
August 24, 2013
Publication Date
December 18, 2001
Subject Category
Instrumentation And Photography
Report/Patent Number
Patent Application Number: US-PATENT-APPL-SN-303725
Patent Number: US-PATENT-6,331,075
Funding Number(s)
CONTRACT_GRANT: NGT-1-52122
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.
Patent
US-PATENT-6,331,075
Patent Application
US-PATENT-APPL-SN-303725
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