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Dynamic refractometerA refractometer computer controls the rotation of a rotary plate upon which are mounted a prism optically coupled via an optical window to a spectroscopic cell holding a resin exhibiting a dynamic refractive index during photocuring. The computer system positions the prism and spectroscopic cell relative to a visible light laser which illuminates the prism-resin interface at selected incidence angles. A photodetector mounted on the plate generates a signal to the computer proportional to intensity of an internally reflected light beam. A curing light is selectively transmitted through the prism and into the photocurable resin. The refractometer determines the intensity of the internally reflected beam a selected incidence angles and determines the effective refractive index curve of the resin at an uncured state and, optionally, at a completely cured state. Next, an amount of uncured resin and selected optical components to be joined by the resin is placed in the spectroscopic cell and irradiated with the UV light. The refractometer is fixed at a selected incidence angle and measures the intensity of an internally reflected light beam of light throughout the cure cycle. The refractometer determines the resin's refractive index of the polymeric mixture by means of extrapolation of a horizontal shift in the effective refractive index curve of the resin from an uncured state to a selected point in the cure cycle.
Document ID
20090004213
Acquisition Source
Marshall Space Flight Center
Document Type
Other - Patent
Authors
Curley, Michael J.
Sarkisov, Sergey S.
Date Acquired
August 24, 2013
Publication Date
November 25, 2008
Subject Category
Optics
Report/Patent Number
Patent Number: US-Patent-7,456,942
Patent Application Number: US-Patent-Appl-SN-11/582,625
Funding Number(s)
CONTRACT_GRANT: NAG8-1880
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.
Patent
US-Patent-7,456,942
Patent Application
US-Patent-Appl-SN-11/582,625
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