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Synthesis of N-Substituted Silaneamines: Monomeric Precursors of Silicon Carbide-Nitride FibersSilanetriamines are prepared by the condensation of methyl or phenyl trichlorosilane with a primary amine. The amines used were methyl, n-propyl, n-butyl and allyl. The silaneamines were prepared by adding the chlorosilane to a solution of the amine in either petroleum ether or toluene. The compounds were purified by distillation and characterized by infrared and nuclear magnetic resonance spectroscopy.
Document ID
19840007965
Acquisition Source
Legacy CDMS
Document Type
Other
Authors
Crouse, D. J.
(Tennessee Technological Univ. Cookeville, TN, United States)
Date Acquired
August 12, 2013
Publication Date
December 1, 1983
Publication Information
Publication: Alabama Univ. Res. Rept.: 1983 NASA(ASEE Summer Faculty Fellowship Program
Subject Category
Nonmetallic Materials
Accession Number
84N16033
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.
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