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Fluoride glass starting materials - Characterization and effects of thermal treatmentThe production of heavy metal fluoride (HMF) glasses, and the effects of thermal treatments on the HMF glasses are investigated. ZrF4, BaF2, AlF3, LaF3, and NaF were utilized in the synthesis of zirconium-barium-lanthanum-aluminum-sodium fluoride glass. The purity of these starting materials, in particular ZrF4, is evaluated using XRD analysis. The data reveal that low temperature heating of ZrF4-H2O is effective in removing the water of hydration, but causes the production of ZrF4 and oxyfluorides; however, dehydration followed by sublimation results in the production of monoclinic ZrFe without water or oxyfluoride contaminants.
Document ID
19880033537
Document Type
Reprint (Version printed in journal)
External Source(s)
Authors
Chen, William
(California Univ. Los Angeles, CA, United States)
Dunn, Bruce
(California, University Los Angeles, United States)
Shlichta, Paul
(California Univ. Los Angeles, CA, United States)
Neilson, George F.
(California Univ. Los Angeles, CA, United States)
Weinberg, Michael C.
(California Institute of Technology Jet Propulsion Laboratory, Pasadena, United States)
Date Acquired
August 13, 2013
Publication Date
October 1, 1987
Publication Information
Publication: Journal of Materials Science Letters
Volume: 6
ISSN: 0261-8028
Subject Category
Nonmetallic Materials
Accession Number
88A20764
Distribution Limits
Public
Copyright
Other

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