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Stationary Crystal Diffraction with a Monochromatic Convergent X-Ray Source and Application for Macromolecular Crystal Data CollectionA diffraction geometry utilizing convergent X-rays from a polycapillary optic incident on a stationary crystal is described. A mathematical simulation of the resulting diffraction pattern (in terms of spot shape, position and intensity) is presented along with preliminary experimental results recorded from a lysozyme crystal. The effective source coverage factor is introduced to bring the reflection intensities onto the same scale. The feasibility of its application to macromolecular crystal data collection is discussed.
Document ID
19980227537
Acquisition Source
Headquarters
Document Type
Reprint (Version printed in journal)
Authors
Ho, Joseph X.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Snell, Eddie H.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Sisk, R. Charles
(NASA Marshall Space Flight Center Huntsville, AL United States)
Ruble, John R.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Carter, Daniel C.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Owens, Scott M.
(Albany Univ. Albany, NY United States)
Gibson, Walter M.
(Albany Univ. Albany, NY United States)
Date Acquired
August 18, 2013
Publication Date
January 1, 1998
Publication Information
Publication: Acta Crystallographics
Publisher: International Union of Crystallography
Issue: Secti D54
ISSN: 0907-4449
Subject Category
Solid-State Physics
Funding Number(s)
CONTRACT_GRANT: NAS8-39926
PROJECT: RTOP 963-40-08
Distribution Limits
Public
Copyright
Other

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