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Stationary Crystal Diffraction with a Monochromatic Convergent X-Ray Source and Application for Macromolecular Crystal Data CollectionA diffraction geometry utilizing convergent X-rays from a polycapillary optic incident on a stationary crystal is described. A mathematical simulation of the resulting diffraction pattern (in terms of spot shape, position and intensity) is presented along with preliminary experimental results recorded from a lysozyme crystal. The effective source coverage factor is introduced to bring the reflection intensities onto the same scale. The feasibility of its application to macromolecular crystal data collection is discussed.
Document ID
19990019565
Acquisition Source
Marshall Space Flight Center
Document Type
Other
Authors
Ho, J. X.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Snell, E. H.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Sisk, R. C.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Ruble, J. R.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Carter, D. C.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Owens, S. M.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Gibson, W. M.
(NASA Marshall Space Flight Center Huntsville, AL United States)
Date Acquired
August 19, 2013
Publication Date
January 1, 1997
Publication Information
Publication: Acta Crystallographica, Section D
Subject Category
Solid-State Physics
Distribution Limits
Public
Copyright
Work of the US Gov. Public Use Permitted.

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