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Synthesis of stereospecifically deuterated desoxypodophyllotoxins and 1H-nmr assignment of desoxypodophyllotoxin[4 beta- 2H1]Desoxypodophyllotoxin [3], [4 alpha- 2H1]desoxypodophyllotoxin [4], and [4, 4- 2 H2]desoxypodophyllotoxin [9] were prepared from podophyllotoxin [1] via its chloride [5]. A complete assignment of the 1H-nmr spectrum of desoxypodophyllotoxin [2] was made on the basis of the spectra of the deuterated compounds [3] and [4].
Document ID
20040112254
Acquisition Source
Legacy CDMS
Document Type
Reprint (Version printed in journal)
External Source(s)
Authors
Pullockaran, A. J.
(Virginia Polytechnic Institute and State University Blacksburg 24061-0212)
Kingston, D. G.
Lewis, N. G.
Date Acquired
August 21, 2013
Publication Date
November 1, 1989
Publication Information
Publication: Journal of natural products
Volume: 52
Issue: 6
ISSN: 0163-3864
Subject Category
Life Sciences (General)
Funding Number(s)
CONTRACT_GRANT: 86-FSTY-9-0188
Distribution Limits
Public
Copyright
Other
Keywords
NASA Discipline Number 29-20
NASA Program Space Biology
NASA Discipline Plant Biology
Non-NASA Center

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